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1H NMR characterization of renatured lysozyme obtained from fully reduced lysozyme under folding/oxidation conditions: A high resolution liquid NMR study at magic angle spinning

Abstract : Magic angle spinning (MAS) has long been used as a powerful technique in studies of heterogeneous samples such as powdered solids, compartmentalized liquids and heterogeneous solid-liquid mixtures. Recently it has been shown that higher resolution could be achieved if high-resolution magnetic susceptibility matching probe technology was used in conjunction with MAS (Nano-probe). In this paper the possibilities and advantages of generating high-resolution spectra of liquids is illustrated using the Nano.nmr probe for the study in solution of lysozyme subjected to various treatments.
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Submitted on : Wednesday, April 1, 2009 - 3:25:29 PM
Last modification on : Wednesday, May 27, 2020 - 7:42:02 AM

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Muriel Delepierre, Pascale Roux, Michel Goldberg, Alain Chaffotte. 1H NMR characterization of renatured lysozyme obtained from fully reduced lysozyme under folding/oxidation conditions: A high resolution liquid NMR study at magic angle spinning. Magnetic Resonance in Chemistry, Wiley, 1998, pp.645-650. ⟨10.1002/(SICI)1097-458X(199809)36:9<645::AID-OMR353>3.0.CO;2-P⟩. ⟨pasteur-00372567⟩

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